we have an instrument that has recently been installed and I would like to create a new instrument model. I have collected capillary data on a NIST std (silicon) and will use this to refine the instrument parameters.
I have been asked about the procedure to follow when doing this, and it struck me that I have never been instructed or read a 'standard' (if there is such a thing) procedure to follow when doing this. For example, is there a 'correct' order to refine and fix parameters etc.
If anyone here is aware of a set procedure for the generation of an instrument model, or that would be happy to share the procedures that you use yourself, it would be geat to find out