I'm trying to do a quantification of both the
NIST SRM656 samples.
After my first go, I'm getting significantly negative amorphous content for the high-alpha (using 676 as an internal std at 10%).
I'm trying to copy the analysis approach outlined in the NST certificate, but the structures they used don't have thermal parameters given in the papers.
Does anybody have any inside information on the actual parameters used in the analyses?
Matthew